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Emissions Test Methods List

Air Pollution Testing personnel have performed virtually all EPA source emissions test methods, as well as a number of methods published through other sources.  Additionally, APT personnel continue to work with regulatory and laboratory personnel to adapt and/or develop new methods for our clients= needs.  The following section details some of the test methods which APT personnel have conducted over the years.

 

40 CFR Part 60, Appendix A Test Methods

 C         Methods 1, 2 (A,B,C,D,F,G,H) : Gas Flow, including 3-D and wall effects

C         Method 3 (A,B) : O2/CO2 by Fyrite, Orsat and Instrumental Analyzer

C         Method 4 : Moisture

C         Method 5 (B,D,F) : Particulate Matter including Positive Pressure Fabric Filter

C         Methods 6 and 6C : Sulfur Dioxide (wet chemical and instrumental procedures)

C         Method 7E : Nitrogen Oxides

C         Method 8 : Sulfur Dioxide, Sulfur Trioxide and Sulfuric Acid Mist

C         Method 9 : Visual Determination of Opacity

C         Method 10 : Carbon Monoxide

C         Method 11 : Hydrogen Sulfide

C         Method 12 : Inorganic Lead

C         Method 13B : Total Fluoride

C         Method 16 : Total Reduced Sulfur (GC / flame photometric detection)

C         Method 17 : Particulate Matter (in-stack filter)

C         Method 18 : Speciated Organic Compounds (GC / flame ionization detection)

C         Method 19 : Stoichiometric Calculation of Gas Flow Rate

C         Method 20 : Nitrogen Oxides and Sulfur Dioxide Emissions from Turbines

C         Method 21 : Determination of Volatile Organic Compounds Leaks

C         Method 22 : Visual Determination of Particulate Emissions from Flares

C         Method 23 : Polychlorinated Dibenzo-p-dioxins, Polychlorinated Dibenzofurans

C         Method 25 (A,C) : Volatile Organic Compounds (flame ionization detection)

C         Method 26 and 26A : Hydrogen Chloride (and other hydrogen halides and halogens)

C         Method 29 : Multiple Metals

 

40 CFR Part 51, Appendix M Test Methods

 C         Method 201A : PM10 (particulate matter less than 10 microns in diameter)

C         Method 202 : Condensible Particulate Matter

 

SW-846 Test Methods

C         Method 0010 : Semi-volatile Organic Compounds (GC / mass spectroscopy)

C         Method 0011 : Aldehydes and Ketones (high performance liquid chromatography)

C         Method 0012 : Multiple Metals

C         Method 0013 : Hexavalent Chromium (Modified EPA Method 306)

C         Method 0030 : Volatile Organic Compounds (GC / mass spectroscopy)

C         Method 0040 : Total Chromatographable Organics

C         Method 0050 : Hydrogen Chloride and Chlorine

 

Other Test Methods (including Modified and Original Test Methods)

 Organics

C         EPA Method 320 : Vapor Phase Organics by FTIR

C         EPA Method TO-6 : Phosgene

C         EPA Method TO-14 : Toxic Organics (GC / mass spectroscopy)

C         Triethylene Glycol using Gas Chromatography / Flame Ionization Detection

C         BTEX (benzene, toluene, ethylbenzene and xylenes) at % (and ppm / ppb) level

C         VOC, BTEX, Hexane from glycol dehydrator using rich/lean glycol mass balance

C         Formaldehyde using Ion Chromatography

C         Formaldehyde using on-site Colorimetry (Modified Celanese Method)

 Inorganics

C         EPA Method 022 : Nitrogen Oxides with an Electrochemical Analyzer

C         EPA Method CTM-027 : Ammonia

C         EPA Method 206 : Ammonia

C         EPA Method 306 : Hexavalent and Total Chromium

C         EPA Method 321 : Vapor Phase Hydrogen Chloride by FTIR

C         Modified NIOSH Method 6001 : Arsine

C         Modified NIOSH Method 7904 : Hydrogen Cyanide

C         Modified CARB 426 : Hydrogen Cyanide

C         BAAQMD (Bay Area Air Quality Management District) Method ST-1B : Ammonia

C         Nitrogen Dioxide using Long-Pathlength Infrared spectroscopy

C         Nitrogen and Hydrogen using Thermal Conductivity Detection

C         Carbon Monoxide (and other pollutants) at % level using dilution system

C         Ontario Hydro Method for speciated mercury

 

Particle Size Analysis

C         Particle Size Distribution using Electrozone and/or Bahco analysis

C         Particle Size Distribution using a Cascade Impactor

                        

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Last modified: 10/27/07